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ISO 3071-2020 pdf free download
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ISO 3071-2020 pdf free download.Textiles一Determination ofpH of aqueous extract.
6 Apparatus
6.1 Stoppered glass or polypropylene flasks, chemically resistant, for preparation of the aqueous extract.
It is recommended that the glassware used for this test be set aside for this purpose only.
6.2 Mechanical shaker, providing rotational or reciprocating movement sufficient to obtain a ready exchange of liquid between the interior of the textile material and the solution used in preparing the extract. A to-and-fro movement at a rate of 60 r/min or a rotational frequency of 30 r/min has been found satisfactory.
6.3 Beakers, chemically resistant, with a capacity of 150 ml (see 6Jj.
6.4 Rods, chemically resistant (see J.).
6.5 pH-meter. with a glass electrode, with a resolution of at least 0.01 pH-units. A pH-meter with temperature compensation is recommended.
6.6 Balance, with a resolution of at least 0,01 g.
6.7 1 I volumetric flasks, of grade A quality.
7 Preparation of test specimens
Take a laboratory test sample representative of the bulk of the textile material and sufficient to provide all the test specimens required. Cut the laboratory test sample into pieces having approximately 5 mm sides or of such a size as to allow the test specimens to wet out rapidly.
To avoid contamination, handle the material as little as possible. Take from the laboratory test sample two test specimens of (2,00 ± 0,05) g each.
8 Procedure
8.1 Preparation of the aqueous extract
Prepare the extract of each test specimen at room temperature as follows.
Place each test specimen and 100 ml of extracting solution Ipotassium chloride solution (5.2)I into a stoppered flask (f.1). Agitate the flask for a short period by hand to ensure that the textile material is properly wetted out, then shake it mechanically (62) for 2 h ± 5 mm.
8.2 Measurement of the pH of the aqueous extract Record the temperature o the extracting solution used.
Calibrate the pH-meter, according to the manufacturer instructions, at the temperature of the extract to be measured. Check the calibration of the pH-meter using two buffer solutions.ISO 3071 pdf download.


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