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ISO 13503-1-2011 pdf download
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ISO 13503-1-2011 pdf download.Petroleum and natural gas industries – Completion fluids and materials – Part 1: Measurement of viscous properties of completion fluids.
3 Measurement and precision
Temperatures shall be measured to an accuracy of ±1 °C (±2 °F); pH shall be measured to an accuracy of ±0,1
units. All other quantitative measurements shall be made to an accuracy of ±2 %, unless specified otherwise.
4 Fluid preparation
Certain aspects of sample preparation and handling can affect the viscosity or rheological properties of a fluid. During all procedures, steps shall be taken to minimize entraining air into the fluid.
The procedure used to prepare the fluid sample shall be documented, including the following information:
a) description and/or composition of the base fluid; preparation of the fluid shall be described, starting with the fluid source, such as deionized water, tap water, completion brines, produced water, seawater or type of oil:
b) identification of mixing apparatus, container volume, and total volume of fluid prepared;
C) identification of each fluid component and amount added;
d) the order and method of addition of each component;
e) mixing speeds, with time at each speed;
f) ageing or holding time prior to measurements, if required;
g) temperature;
h) pH (for aqueous fluids);
i) all other aspects of the fluid preparation which are known to affect the outcome of the viscosity measurement, such as filtration of completion fluids.
5 Fluid preparation using shear-history simulation (optional)
5.1 General
A shear-history simulation procedure is provided to simulate the effects of shear rate and time while a fluid is being conveyed down well tubulars. This procedure is intended to characterize the effect of shear history on fluid properties as part of the concept and development phase for a new fluid.
A shear-history apparatus is used to condition the fluid at specified shear rates, times and temperatures prior to injection into a viscometer. It consists of mixing apparatus, pumping apparatus and tubing to simulate significant aspects of the surface apparatus followed by shear conditions in the well tubulars. A shear-history apparatus that satisfies the requirements can be generically classified as a tube or pipe flow device that operates in the laminar flow regime. Flow shall occur in a single-pass mode.
A schematic diagram of a shear-history simulator connected to a pressurized concentric-cylinder viscometer is shown in Figure 1. In laminar flow, the energy dissipation rate is the same in any shear-history apparatus even if different tubing sizes are used. Thus, the design and functioning of the apparatus can vary and still meet the desired precond itioning criteria.ISO 13503-1 pdf download.


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