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AS 1289.4.3.1:2021 pdf free download
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AS 1289.4.3.1:2021 pdf free download.Methods of testing soils for engineering purposes Method 4.3.1: Soil chemical tests – Determination of the pH value of a soil – Electrometric method.
AS 1289.4.3.1 covers the electrometric determination of the pH value of a soil-suspension.
NOTE The pH value a sample groundwater can be measured in a similar manner to that used for a
soil-suspension.
2 Normative references
The following documents are referred to in the text in such a way that some or all of their content constitutes requirements of this document.
NOTE Documents referenced for informative purposes are listed in the Bibliography.
AS 1289.1.1, Methods of testing soils for engineering purposes, Method 1.1: Preparation of disturbed soil samples for testing
ISO 3310-2, Test sieves — Technical requirements and testing — Part 2: Test sieves of perforated metal plate
3 Terms and definitions
No terms and definitions are listed in this document.
4 Apparatus
The following apparatus are required:
(a) pH meter, covering at least the range pH 3.0 to pH 13.0, fitted with a scale that is readable and accurate to 0.05 pH units.
NOTE 1 Soils with high p11 values, such as stabilized soils and naturally occurring soils with a pH in excess of 10, should use an electrode reading to pH 13.0 as other electrodes would be adversely affected.
NOTE 2 The pH meter manufacturer’s instructions should be followed.
(b) Balance of at least 100 g capacity, with a limit of performance not greater than ± 0.05g.
(c) 100 mL glass beakers, with cover glasses and stirring rods.
(d) Wash-bottle, preferably plastic, containing distilled water.
(e) 2.36 mm sieve, conforming to ISO 3310-2.
(f) Thermometer, readable and accurate to 1 °C
5 Reagents
The following reagents of analytical reagent (AR) grade are required:
(a) Buffer solutions — p11 40. pH 9.2 and other pH levels within 2 pH units of the soil being measured as required.
(b) Potassium chloride — Saturated solution, for maintenance of calomel electrode.
(c) Distilled water — pH of between 6.75 and 7.25. stored in a sealed container.
6 Procedure
Tests shall be performed within the temperature range of 15 °C to 25 °C.
The procedure shall be as follows:
(a) Obtain a sample which has been prepared in accordance with the procedure for the preparation of disturbed samples for testing specified in AS 1289.1.1. Remove all particles by sieving over the 2.36 mm sieve. Do not oven dry the sample.
By riffling or quartering, obtain a sample of about 35 g from the material passing the sieve. NOTE 1 The soil should be sufficiently dry so that It will pass the sieve.
NOTE 2 The preparation the sample from either an air-dried or natural state will produce different results. Therefore, it is recommended that samples are tested in the natural state.
(b) Transfer 30 ± 0.Olg of the sample into a 100 mL beaker and add 75 ± 0.05 g of distilled water. The temperature of the water shall be in equilibrium with the testing environment before commencing the test.
Stir the suspension regularly in the first 30 mm, then cover the beaker with a cover glass and allow it to stand for at least 60 mm.
NOTE 3 Highly plastic clays can require longer saturation to break up the clay particles.
NOTE 4 For stabilized soils, the standing time should be not more than 2h, otherwise irreversible changes can take place in the stabilizers.
(c) Calibrate the pH meter using standard buffer solutions, in accordance with the manufacturer’s procedures.AS 1289.4.3.1 pdf download.


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